SYNTHESIS AND CHARACTERIZATION OF (2E)-1-{4-[2,4-DITHIO-3-(2-METHYLPROPAN-2-YL)IMINO-5-SUBSTITUTEDIMINO-1,3,5-TRIAZINO-6-YL] AMINOPHENYL}-3-(3,4-DIMETHOXYPHENYL)PROP-2-EN-1-ONE

Dipak T. Tayade* and Siddharth A. Waghmare

ABSTRACT

Recently, in the laboratory isomerisation of series of (2E)-1-{4-[2-(2-methylpropan-2-yl) imino-4-substitutedimino) amino-1,3,5-dithiazino-6-yl] aminophenyl}-3-(3,4-dimethoxy phenyl)prop-2-en-1-one (Ia-e) were carried using sodium bicarbonate in aqueous ethanol in to (2E)-1-{4-[2,4-dithio-3-(2-methylpropan-2-yl)-5-substituted-1,3,5-triazino-6-yl] amino phenyl}-3-(3,4-dimethoxyphenyl)prop-2-en-1-one (IIa-e). The structure of all the synthesized compounds was justified on the basis of chemical tests, elemental data and spectral characterization.

Keywords: (2E)-1-{4-[2-(2-methylpropan-2-yl) imino-4-substitutedimino) amino-1,3,5-dithiazino-6-yl] aminophenyl}-3-(3,4-dimethoxyphenyl) prop-2-en-1-one (Ia-e), sodium bicarbonate, ethanol and spectral Characterization etc.